Nanocrystalline titanium dioxide catalyst for the synthesis of azlactones

doi:10.1016/S1872-2067(12)60741-4

催化学报 ›› 2014, Vol. 35 ›› Issue (2): 196-200.DOI: 10.1016/S1872-2067(12)60741-4

Nanocrystalline titanium dioxide catalyst for the synthesis of azlactones

Priyanka Anandgaonker, Ganesh Kulkarni, Suresh Gaikwad, Anjali Rajbhoj

Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad 431004 (MS), India

收稿日期:2013-08-25 修回日期:2013-10-21 出版日期:2014-01-16 发布日期:2014-01-17
通讯作者: Anjali Rajbhoj

Nanocrystalline titanium dioxide catalyst for the synthesis of azlactones

Priyanka Anandgaonker, Ganesh Kulkarni, Suresh Gaikwad, Anjali Rajbhoj

Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad 431004 (MS), India

Received:2013-08-25 Revised:2013-10-21 Online:2014-01-16 Published:2014-01-17
Contact: Anjali Rajbhoj

摘要/Abstract

摘要：

Titanium dioxide nanoparticles were prepared by a electrochemical reduction method using parameters such as current density, solvent polarity, distance between electrodes, and concentration of stabilizers to control the size of the nanoparticles. The nanoparticles were characterized by UV-Vis spectroscopy, X-ray diffraction, scanning electron microscopy and transmission electron microscopy, and their catalytic performance was tested for the synthesis of a series of 4-aryldiene-2-phenyl-5(4)-oxazolones from the cyclodehydration and condensation of the respective aldehyde, hippuric acid and acetic anhydride. Easy availability, reusability and eco-friendliness were some prominent features of the nanocrystalline titanium dioxide catalyst.

关键词: Nanocrystalline titanium dioxide, Electrochemical reduction method, Cyclodehydration-condensation, Heterogeneous catalyst

Abstract:

Key words: Nanocrystalline titanium dioxide, Electrochemical reduction method, Cyclodehydration-condensation, Heterogeneous catalyst

Priyanka Anandgaonker, Ganesh Kulkarni, Suresh Gaikwad, Anjali Rajbhoj. Nanocrystalline titanium dioxide catalyst for the synthesis of azlactones[J]. 催化学报, 2014, 35(2): 196-200.

Priyanka Anandgaonker, Ganesh Kulkarni, Suresh Gaikwad, Anjali Rajbhoj. Nanocrystalline titanium dioxide catalyst for the synthesis of azlactones[J]. Chinese Journal of Catalysis, 2014, 35(2): 196-200.

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Nanocrystalline titanium dioxide catalyst for the synthesis of azlactones

Nanocrystalline titanium dioxide catalyst for the synthesis of azlactones

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