Chemical vapor deposition of Pd(C3H5)(C5H5) for the synthesis of reusable Pd@ZIF-8 catalysts for the Suzuki coupling reaction

doi:10.1016/S1872-2067(14)60292-8

Abstract

Abstract:

A zeolite-imidazolium-framework-supported Pd-based heterogeneous catalyst (Pd@ZIF-8) was prepared by a metal-organic chemical vapor deposition method under mild conditions using Pd(C₃H₅)(C₅H₅) as the Pd precursor. N₂ adsorption and pore size distribution data showed that ZIF-8 and Pd@ZIF-8 both possessed high surface areas. Transmission electron microscopy images showed that Pd nanoparticles with sizes of about 1.5-3.5 nm were homogeneously dispersed on the ZIF-8 support in Pd@ZIF-8. The Pd@ZIF-8 catalyst showed good activity in Suzuki coupling reactions with several different kinds of aryl halides. It could be reused at least six times without dramatic loss of activity or decomposition of the ZIF-8 structure.

Key words: Palladium, ZIF-8, Metal-organic chemical vapor deposition, Suzuki coupling reaction

Mingming Zhang, Ya Gao, Chuang Li, Changhai Liang. Chemical vapor deposition of Pd(C₃H₅)(C₅H₅) for the synthesis of reusable Pd@ZIF-8 catalysts for the Suzuki coupling reaction[J]. Chinese Journal of Catalysis, 2015, 36(4): 588-594.

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Chemical vapor deposition of Pd(C₃H₅)(C₅H₅) for the synthesis of reusable Pd@ZIF-8 catalysts for the Suzuki coupling reaction

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