Preparation and application of highly efficient Au/SnO2 catalyst in the oxidative lactonization of 1,4-butanediol to γ-butyrolactone

doi:10.1016/S1872-2067(12)60534-8

Abstract

Abstract:

A series of gold catalysts supported on commercial SnO₂ were synthesized by deposition-precipitation while accurately controlling pH and precipitant species. The supported catalysts were characterized by X-ray diffraction, inductively coupled plasma atomic emission spectrometry, transmission electron microscopy, and X-ray photoelectron spectroscopy. Gold loading and calcination temperature both affected the dispersion and nature of gold species on SnO₂. The performance of the catalysts in the oxidative lactonization of 1,4-butanediol to g-butyrolactone was investigated. The catalyst with 3% gold that was calcined at 573 K exhibited the highest activity, which was 15 times higher than that of Au/TiO₂. The excellent catalytic performance was attributed to the high dispersion of gold particles and adequate Au⁰ and Au^δ^- species formed because of the strong interaction between Au and SnO₂ and the intrinsic properties of SnO₂.

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Key words: Gold catalyst, Tin dioxide, Deposition-precipitation method, 1,4-Butanediol, Oxidative lactonization, Calcination temperature, Gold loading

LI Xian, ZHENG Jiamin, YANG Xinli, DAI Weilin, FAN Kangnian. Preparation and application of highly efficient Au/SnO₂ catalyst in the oxidative lactonization of 1,4-butanediol to γ-butyrolactone[J]. Chinese Journal of Catalysis, 2013, 34(5): 1013-1019.

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https://www.cjcatal.com/EN/Y2013/V34/I5/1013

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Preparation and application of highly efficient Au/SnO₂ catalyst in the oxidative lactonization of 1,4-butanediol to γ-butyrolactone

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