Propene and CO oxidation on Pt/Ce-Zr-SO42- diesel oxidation catalysts: Effect of sulfate on activity and stability

doi:10.1016/S1872-2067(17)62781-5

Abstract

Abstract:

Platinum/cerium-zirconium-sulfate (Pt/Ce-Zr-SO₄^2-) catalysts were prepared by wetness impregnation. Catalytic activities were evaluated from the combustion of propene and CO. Sulfate (SO₄^2-) addition improved the catalytic activity significantly. When using Pt/Ce-Zr-SO₄^2- with 10 wt% SO₄^2-, the temperature for 90% conversion of propene and CO decreased by 75℃ compared with Pt/Ce-Zr. The conversion exceeded 95% at 240℃ even after 0.02% sulfur dioxide poisoning for 20 h. Temperature-programmed desorption of CO and X-ray photoelectron spectroscopy analyses revealed an improvement in Pt dispersion onto the Ce-Zr-SO₄^2- support, and the increased number of Pt particles built up more Pt^&+-(SO₄^2-)^&- couples, which resulted in excellent activity. The increased total acidity and new Brönsted acid sites on the surface provided the Pt/Ce-Zr-SO₄^2- with good sulfur resistance.

Key words: Diesel oxidation catalyst, Pt/Ce-Zr-SO₄^2- catalyst, Sulfur resistance, Catalytic oxidation

Lei Gu, Xiao Chen, Ying Zhou, Qiulian Zhu, Haifeng Huang, Hanfeng Lu. Propene and CO oxidation on Pt/Ce-Zr-SO₄^2- diesel oxidation catalysts: Effect of sulfate on activity and stability[J]. Chinese Journal of Catalysis, 2017, 38(3): 607-616.

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Propene and CO oxidation on Pt/Ce-Zr-SO₄^2- diesel oxidation catalysts: Effect of sulfate on activity and stability

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