Ni/Al2O3 catalysts derived from spinel NiAl2O4 for low-temperature hydrogenation of maleic anhydride to succinic anhydride

doi:10.1016/S1872-2067(17)62844-4

Abstract

Abstract:

Ni/Al₂O₃ catalysts were derived from spinel NiAl₂O₄ with different Ni content ((2.5, 5 and 7.5) wt%). The catalysts were obtained by H₂ reduction and were investigated for the low-temperature hydro-genation of maleic anhydride (MA) to produce succinic anhydride (SA). The characterization results showed that Ni⁰ active sites were mainly derived during the H₂ reduction from spinel NiAl₂O₄. Among the catalysts studied, employing the optimum preparation and reaction conditions with Ni(5%)/Al₂O₃ yielded the highest catalytic performance. A near-100% conversion of MA and~90% selectivity to SA were achieved at 120℃ and 0.5 MPa of H₂ with a weighted hourly space velocity (MA) of 2 h^-1.

Key words: Maleic anhydride, Succinic anhydride, Hydrogenation, Nickel, Spinel

Jie Li, Yuanhang Ren, Bin Yue, Heyong He. Ni/Al₂O₃ catalysts derived from spinel NiAl₂O₄ for low-temperature hydrogenation of maleic anhydride to succinic anhydride[J]. Chinese Journal of Catalysis, 2017, 38(7): 1166-1173.

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Ni/Al₂O₃ catalysts derived from spinel NiAl₂O₄ for low-temperature hydrogenation of maleic anhydride to succinic anhydride

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