Solid-state CTAB-assisted synthesis of mesoporous Fe3O4 and Au@Fe3O4 by mechanochemistry

doi:10.1016/S1872-2067(19)63288-2

Abstract

Abstract:

Mesoporous iron oxides have shown excellent performance in many research areas such as catalysts, biosensors, enzyme immobilization, heavy metal adsorption, and drug delivery. The state-of-the-art synthesis methods are mostly wet chemistry processes. This paper reports a solvent-free approach for the rapid synthesis of mesoporous Fe₃O₄ (specific surface area up to 170 m²/g) and Au@Fe₃O₄ (highly dispersed Au nanoparticles, average particle size:~4 nm). With different amounts of added template agent, cetyltrimethylammonium bromide (CTAB), the pore structure could easily be adjusted. More importantly, the mesoporous Fe₃O₄ exhibited good catalytic activity in carbon monoxide (CO) oxidation, outperforming commercially purchased Fe₃O₄ with 100% CO conversion at around 274℃ vs. 490℃ for the commercial product.

Key words: Mechanochemistry, Mesoporous material, Mesoporous catalyst, Carbon monoxide oxidation, Iron oxide

Jiahua Zhao, Yuan Shu, Pengfei Zhang. Solid-state CTAB-assisted synthesis of mesoporous Fe₃O₄ and Au@Fe₃O₄ by mechanochemistry[J]. Chinese Journal of Catalysis, 2019, 40(7): 1078-1084.

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URL: https://www.cjcatal.com/EN/10.1016/S1872-2067(19)63288-2

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Solid-state CTAB-assisted synthesis of mesoporous Fe₃O₄ and Au@Fe₃O₄ by mechanochemistry

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