Layered double hydroxide-like Mg3Al1-xFex materials as supports for Ir catalysts:Promotional effects of Fe doping in selective hydrogenation of cinnamaldehyde

doi:10.1016/S1872-2067(18)63042-6

Abstract

Abstract:

Supported Ir catalysts were prepared using layered double hydrotalcite-like materials, such as Mg₃Al_1-xFe_x, containing Fe and Al species in varying amounts as supports. These Ir catalysts were applied for the selective hydrogenation of cinnamaldehyde (CAL). When x was changed from 0 (Ir/Mg₃Al) to 1 (Ir/Mg₃Fe), the rate of CAL hydrogenation reached a maximum at approximately x=0.25, while the selectivity to unsaturated alcohol, i.e., cinnamyl alcohol, monotonously increased from 44.9% to 80.3%. Meanwhile, the size of the supported Ir particles did not change significantly with x, remaining at 1.7 ±0.2 nm, as determined by transmission electron microscopy. The chemical state of Ir and Fe species in the Ir/Mg₃Al_1-xFe_x catalysts was examined by temperature programmed reduction by H₂ and X-ray photoelectron spectroscopy. The surface of the supported Ir particles was also examined through the in-situ diffuse reflectance infrared Fourier-transform of a probe molecule of CO. On the basis of these characterization results, the effects of Fe doping to Mg₃Al on the structural and catalytic properties of Ir particles in selective CAL hydrogenation were discussed. The significant factors are the electron transfer from Fe²⁺ in the Mg₃Al_1-xFe_x support to the dispersed Ir particles and the surface geometry.

Key words: Ir catalyst, Layered double hydroxide, Fe doping, Support effect, Selective hydrogenation, Cinnamaldehyde

Weiwei Lin, Haiyang Cheng, Xiaoru Li, Chao Zhang, FengyuZhao, Masahiko Arai. Layered double hydroxide-like Mg₃Al_1-xFe_x materials as supports for Ir catalysts:Promotional effects of Fe doping in selective hydrogenation of cinnamaldehyde[J]. Chinese Journal of Catalysis, 2018, 39(5): 988-996.

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Layered double hydroxide-like Mg₃Al_1-xFe_x materials as supports for Ir catalysts:Promotional effects of Fe doping in selective hydrogenation of cinnamaldehyde

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