Preparation of Sn-β-zeolite via immobilization of Sn/choline chloride complex for glucose-fructose isomerization reaction

doi:10.1016/S1872-2067(17)62754-2

Abstract

Abstract:

Well dispersion of tin species in an isolated form is a quite challenge since tin salts are easily hydrolyzed into (hydr)oxides during aqueous stannation of β-zeolite. In this study, immobilization of tin species on high silica commercial β-zeolite by using SnCl₂/Choline chloride (ChCl) complex followed with calcination provided a convenient way to get well dispersed Sn in β-zeolite in the aqueous condition, which was observed based on electron microscopy images, UV visible spectra and X-ray diffraction pattern. The existence of ChCl facilitated tin species to incorporate into zeolite. (1-2) wt% of Sn loaded β-zeolites exhibited good catalytic activity and high selectivity for glucose-fructose isomerization reaction.

Key words: Sn-&beta, zeolite, Immobilization, Choline chloride, Glucose, Isomerization, Fructose

Asep Bayu, Surachai Karnjanakom, Katsuki Kusakabe, Abuliti Abudula, Guoqing Guan. Preparation of Sn-β-zeolite via immobilization of Sn/choline chloride complex for glucose-fructose isomerization reaction[J]. Chinese Journal of Catalysis, 2017, 38(3): 426-433.

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URL: https://www.cjcatal.com/EN/10.1016/S1872-2067(17)62754-2

https://www.cjcatal.com/EN/Y2017/V38/I3/426

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